Technology Process of C18H19NOS2
There total 4 articles about C18H19NOS2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetraphosphorus decasulfide; Hexamethyldisiloxane;
In
1,2-dichloro-benzene;
at 110 ℃;
for 1h;
Microwave irradiation;
Inert atmosphere;
DOI:10.1021/jm3011349
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bis(triphenylphosphine)palladium(II)-chloride; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / 80 °C / Inert atmosphere
2: toluene-4-sulfonic acid / toluene / 16 h / Dean-Stark; Reflux; Inert atmosphere
3: Hexamethyldisiloxane; tetraphosphorus decasulfide / 1,2-dichloro-benzene / 1 h / 110 °C / Microwave irradiation; Inert atmosphere
With
bis(triphenylphosphine)palladium(II)-chloride; tetraphosphorus decasulfide; Hexamethyldisiloxane; sodium carbonate; toluene-4-sulfonic acid;
In
1,2-dimethoxyethane; water; 1,2-dichloro-benzene; toluene;
DOI:10.1021/jm3011349
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / toluene / 16 h / Dean-Stark; Reflux; Inert atmosphere
2: Hexamethyldisiloxane; tetraphosphorus decasulfide / 1,2-dichloro-benzene / 1 h / 110 °C / Microwave irradiation; Inert atmosphere
With
tetraphosphorus decasulfide; Hexamethyldisiloxane; toluene-4-sulfonic acid;
In
1,2-dichloro-benzene; toluene;
DOI:10.1021/jm3011349
