heptacarbonyldiiron

Base Information

• Chemical Name: heptacarbonyldiiron
• CAS No.: 79391-63-2
• Molecular Formula: C₁₇H₁₆As₂Fe₂O₇
• Molecular Weight: 593.847
• Mol file: 79391-63-2.mol

Synonyms:

Chemical Property of heptacarbonyldiiron

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of heptacarbonyldiiron

There total 1 articles about heptacarbonyldiiron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diiron nonacarbonyl (15321-51-4) + ortho-phenylenebis(dimethylarsine) (13246-32-7) → o-phenylenebis(dimethylarsine)Fe2(CO)8 (24996-29-0) + heptacarbonyldiiron (79391-63-2)

Guidance literature:

With CO; In tetrahydrofuran; stirring for 6 h at 25°C with slow stream of carbon monoxide bubbling through the reaction mixture; evapn. under vac., redissolved in hexane and column chromy on silica, elution with 1:1 hexane:benzene, yellow fraction gave after recrystn. from CH2Cl2 and hexane (diars)Fe2(CO)8, red fraction gave (diars)Fe2(CO)7, elem. anal.;

DOI:10.1021/ic00131a054

upstream raw materials:

diiron nonacarbonyl

ortho-phenylenebis(dimethylarsine)