C₂₄H₃₇N₆O₅P

Base Information

Chemical Name:C₂₄H₃₇N₆O₅P
CAS No.:1082741-32-9
Molecular Formula:C₂₄H₃₇N₆O₅P
Molecular Weight:520.569
Hs Code.:

C<sub>24</sub>H<sub>37</sub>N<sub>6</sub>O<sub>5</sub>P

Synonyms:

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Chemical Property of C₂₄H₃₇N₆O₅P

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Technology Process of C₂₄H₃₇N₆O₅P

There total 10 articles about C₂₄H₃₇N₆O₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₅ClN₅O₅P

: 1082741-32-9
C₂₄H₃₇N₆O₅P

Guidance literature:: With ammonia; In methanol; at 85 ℃; for 15h; Autoclave;
DOI:10.1016/j.ijpharm.2010.06.036

Reference yield:

: 1082741-08-9
C₁₄H₁₉NO₃

: 1082741-32-9
C₂₄H₃₇N₆O₅P

Guidance literature:: Multi-step reaction with 8 steps

1.1: palladium on activated charcoal; methanesulfonic acid; hydrogen; acetic acid / ethanol; ethyl acetate

2.1: potassium hydroxide / methanol; water / 3.5 h / 100 °C

3.1: pyridine; dmap / 144 h / Heating

4.1: ethyl methyl ether; water / 16 h / 125 °C

5.1: tetrabutyl-ammonium chloride; N,N-dimethyl-aniline; trichlorophosphate / acetonitrile / 8.5 h / 110 °C

5.2: 15.25 h / 0 °C

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.5 h / 20 °C

6.2: 17 h / 70 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 20 °C

8.1: ammonia / methanol / 15 h / 85 °C / Autoclave

With pyridine; dmap; methanesulfonic acid; palladium on activated charcoal; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; hydrogen; acetic acid; N,N-dimethyl-aniline; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; ethyl methyl ether; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.ijpharm.2010.06.036

Reference yield:

: 1082741-25-0
C₁₂H₁₉NO

: 1082741-32-9
C₂₄H₃₇N₆O₅P

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine; dmap / 144 h / Heating

2.1: ethyl methyl ether; water / 16 h / 125 °C

3.1: tetrabutyl-ammonium chloride; N,N-dimethyl-aniline; trichlorophosphate / acetonitrile / 8.5 h / 110 °C

3.2: 15.25 h / 0 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 17 h / 70 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 20 °C

6.1: ammonia / methanol / 15 h / 85 °C / Autoclave

With pyridine; dmap; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; N,N-dimethyl-aniline; 1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate; In tetrahydrofuran; methanol; ethyl methyl ether; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.ijpharm.2010.06.036