Technology Process of C21H34N2O3S
There total 5 articles about C21H34N2O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; iron; calcium chloride / ethanol / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C
3: triethylamine / dichloromethane
With
lithium aluminium tetrahydride; water; iron; triethylamine; calcium chloride;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.01.099
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C
2: triethylamine / dichloromethane
With
lithium aluminium tetrahydride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.01.099
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrazine / ethanol; water / Reflux
2.1: manganese(IV) oxide / 1,4-dioxane / 20 °C
2.2: 20 °C
2.3: Reflux
3.1: water; iron; calcium chloride / ethanol / Reflux
4.1: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C
5.1: triethylamine / dichloromethane
With
manganese(IV) oxide; lithium aluminium tetrahydride; water; iron; triethylamine; calcium chloride; hydrazine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.01.099
