dicarbonyl(dimethylphenylphosphine)bis(pyridine-2-thionato-NS)molybdenum

Base Information

Chemical Name:dicarbonyl(dimethylphenylphosphine)bis(pyridine-2-thionato-NS)molybdenum
CAS No.:130461-35-7
Molecular Formula:C₂₀H₁₉MoN₂O₂PS₂
Molecular Weight:510.429
Hs Code.:

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Chemical Property of dicarbonyl(dimethylphenylphosphine)bis(pyridine-2-thionato-NS)molybdenum

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Technology Process of dicarbonyl(dimethylphenylphosphine)bis(pyridine-2-thionato-NS)molybdenum

There total 1 articles about dicarbonyl(dimethylphenylphosphine)bis(pyridine-2-thionato-NS)molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 2637-34-5,646031-56-3
pyridine-2-thione

: 672-66-2
Dimethyl(phenyl)phosphine

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 130461-35-7
dicarbonyl(dimethylphenylphosphine)bis(pyridine-2-thionato-NS)molybdenum

Guidance literature:: With CH₃CN; In acetonitrile; refluxing of (Mo(CO)6) in MeCN under N2 for 4 h, addn. of the pyridine ligand, stirring for 12 h at room temp., addn. of PMe2Ph and stirring for 24 h; evapn. (vac.), tlc chromy. on silica gel, elution with light petroleum-CH2Cl2 and recrystn. from CH2Cl2-MeOH; elem. anal.;
DOI:10.1039/DT9900002321