C₄₆H₆₃N₅O₉

Base Information

Chemical Name:C₄₆H₆₃N₅O₉
CAS No.:1353660-79-3
Molecular Formula:C₄₆H₆₃N₅O₉
Molecular Weight:830.034
Hs Code.:

C<sub>46</sub>H<sub>63</sub>N<sub>5</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₄₆H₆₃N₅O₉

Chemical Property:

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Technology Process of C₄₆H₆₃N₅O₉

There total 7 articles about C₄₆H₆₃N₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353660-69-1
C₃₂H₃₉N₅O₇

: 1353660-79-3
C₄₆H₆₃N₅O₉

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; potassium carbonate / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

1.2: pH Ca_. 2

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; water; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; toluene; 2.1: Mitsunobu reaction;
DOI:10.1002/chem.201101978

Reference yield:

: 1353724-28-3
(2S,3R)-methyl 3-(4-cyanophenyl)-2,3-dihydroxypropanoate

: 1353660-79-3
C₄₆H₆₃N₅O₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / -25 - 20 °C / Inert atmosphere

2.1: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C

4.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

5.1: water; potassium carbonate / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

5.2: pH Ca_. 2

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 0 - 20 °C / Inert atmosphere

With hydrogen azide; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 1.1: Mitsunobu reaction / 6.1: Mitsunobu reaction;
DOI:10.1002/chem.201101978

Reference yield:

: 1353660-42-0
(2S,3S)-methyl 3-azido-3-(4-cyanophenyl)-2-hydroxypropanoate

: 1353660-79-3
C₄₆H₆₃N₅O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C

3.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

4.1: water; potassium carbonate / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

4.2: pH Ca_. 2

5.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 5.1: Mitsunobu reaction;
DOI:10.1002/chem.201101978