Technology Process of C57H61NO12
There total 5 articles about C57H61NO12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride; triethylamine;
In
dichloromethane; dimethyl sulfoxide;
at -60 - -30 ℃;
DOI:10.1016/j.carres.2012.03.033
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; triethylamine / methanol / 4 h / 40 °C
2: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 °C
3: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / -78 °C / Molecular sieve
4: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / -60 - -30 °C
With
triethylsilane; oxalyl dichloride; trifluorormethanesulfonic acid; water; sodium hydride; triethylamine;
In
methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
1: Zemplen deacetylation / 4: Swern oxidation;
DOI:10.1016/j.carres.2012.03.033
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / -78 °C / Molecular sieve
2: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / -60 - -30 °C
With
triethylsilane; oxalyl dichloride; trifluorormethanesulfonic acid; triethylamine;
In
dichloromethane; dimethyl sulfoxide;
2: Swern oxidation;
DOI:10.1016/j.carres.2012.03.033
