3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole

Base Information

Chemical Name:3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole
CAS No.:1246736-21-9
Molecular Formula:C₁₂H₁₄N₄O₃S₂
Molecular Weight:326.4
Hs Code.:

Synonyms:

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Chemical Property of 3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole

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Technology Process of 3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole

There total 1 articles about 3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110-62-3
pentanal

: 32909-92-5
sulfametrole

: 1246736-21-9
3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole

Guidance literature:: In ethanol; for 3h; Reflux;
DOI:10.1016/j.molstruc.2010.06.002

Reference yield: 71.0%

: 121714-78-1,24290-40-2,58694-80-7,10025-77-1,64333-00-2
iron(III) chloride hexahydrate

: 1246736-21-9
3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole

: [FeCl₃(3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole)(H₂O)]*3H₂O

Guidance literature:: In ethanol; water; hot soln. of Fe-salt in ethanol-water (1:1) was added to a hot soln. (60°C) of thiadiazole-compound in ethanol-water, the mixt. was stirred under reflux for 1 h; ppt. was filtered, washed with 1:1 ethanol-water mixt. and diethyl ether; elem. anal.;
DOI:10.1016/j.molstruc.2010.06.002

Reference yield: 70.0%

: nickel(II) chloride hexahydrate

: 1246736-21-9
3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole

: [NiCl₂(3-(4'-ethylazomethinobenzene sulphonamide)-4-methoxy-1,2,5-thiadiazole)(H₂O)2]*3H₂O

Guidance literature:: In ethanol; water; hot soln. of Ni-salt in ethanol-water (1:1) was added to a hot soln. (60°C) of thiadiazole-compound in ethanol-water, the mixt. was stirred under reflux for 1 h; ppt. was filtered, washed with 1:1 ethanol-water mixt. and diethyl ether; elem. anal.;
DOI:10.1016/j.molstruc.2010.06.002