C₃₂H₄₀N₂O₅

Base Information

Chemical Name:C₃₂H₄₀N₂O₅
CAS No.:1404380-33-1
Molecular Formula:C₃₂H₄₀N₂O₅
Molecular Weight:532.68
Hs Code.:

C<sub>32</sub>H<sub>40</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₃₂H₄₀N₂O₅

Chemical Property:

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Technology Process of C₃₂H₄₀N₂O₅

There total 13 articles about C₃₂H₄₀N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132464-91-6
4'-isobutyl phenylacetylene

: 1404380-33-1
C₃₂H₄₀N₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1: n-butyllithium / tetrahydrofuran / -78 - 0 °C

2: sodium carbonate / ethanol / 80 °C

3: Iodine monochloride / dichloromethane / 0 °C

4: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 80 °C

5: hydrogen / palladium(II) hydroxide / tetrahydrofuran / 760.05 - 3040.2 Torr

6: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 0 - 20 °C / Phosphate buffer

7: potassium carbonate / N,N-dimethyl-formamide

8: trifluoroacetic acid / chloroform

9: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydrogen; Iodine monochloride; sodium carbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; palladium(II) hydroxide; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 40150-98-9
4-(2-methyl-1-propyl)benzaldehyde

: 1404380-33-1
C₃₂H₄₀N₂O₅

Guidance literature:: Multi-step reaction with 11 steps

1: triphenylphosphine / dichloromethane / 0 °C

2: n-butyllithium / hexane; tetrahydrofuran / -78 °C

3: n-butyllithium / tetrahydrofuran / -78 - 0 °C

4: sodium carbonate / ethanol / 80 °C

5: Iodine monochloride / dichloromethane / 0 °C

6: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 80 °C

7: hydrogen / palladium(II) hydroxide / tetrahydrofuran / 760.05 - 3040.2 Torr

8: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 0 - 20 °C / Phosphate buffer

9: potassium carbonate / N,N-dimethyl-formamide

10: trifluoroacetic acid / chloroform

11: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydrogen; Iodine monochloride; sodium carbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; palladium(II) hydroxide; In tetrahydrofuran; ethanol; hexane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 38861-88-0
4-isobutylbenzoic acid

: 1404380-33-1
C₃₂H₄₀N₂O₅

Guidance literature:: Multi-step reaction with 13 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; acetonitrile

2: diisobutylaluminium hydride / toluene / -78 °C

3: triphenylphosphine / dichloromethane / 0 °C

4: n-butyllithium / hexane; tetrahydrofuran / -78 °C

5: n-butyllithium / tetrahydrofuran / -78 - 0 °C

6: sodium carbonate / ethanol / 80 °C

7: Iodine monochloride / dichloromethane / 0 °C

8: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 80 °C

9: hydrogen / palladium(II) hydroxide / tetrahydrofuran / 760.05 - 3040.2 Torr

10: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 0 - 20 °C / Phosphate buffer

11: potassium carbonate / N,N-dimethyl-formamide

12: trifluoroacetic acid / chloroform

13: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydrogen; Iodine monochloride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; palladium(II) hydroxide; In tetrahydrofuran; ethanol; hexane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; acetonitrile;