[K(18-crown-6)][κ2(P,O)(o-triphenylphosphine monosulphonate))PdMeCl]

Base Information

• Chemical Name: [K(18-crown-6)][κ2(P,O)(o-triphenylphosphine monosulphonate))PdMeCl]
• CAS No.: 1333164-66-1
• Molecular Formula: C₁₂H₂₄KO₆*C₁₉H₁₇ClO₃PPdS
• Molecular Weight: 801.672

Synonyms:

Chemical Property of [K(18-crown-6)][κ2(P,O)(o-triphenylphosphine monosulphonate))PdMeCl]

Chemical Property:

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Technology Process of [K(18-crown-6)][κ2(P,O)(o-triphenylphosphine monosulphonate))PdMeCl]

There total 1 articles about [K(18-crown-6)][κ2(P,O)(o-triphenylphosphine monosulphonate))PdMeCl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

chloromethyl(1,5-cyclooctadiene)palladium(II) + [K(18-crown-6)][o-triphenylphosphine monosulphonate] → [K(18-crown-6)][κ2(P,O)(o-triphenylphosphine monosulphonate))PdMeCl] (1333164-66-1)

Guidance literature:

In dichloromethane; under Ar; phosphine and Pd complex dissolved in CH2Cl2; stirred for 17 hunder absence of light; volatiles removed under vac.; washed with pentane; recrystd. from CH2Cl2by overlaying with pentane; filtered; dried under vac.; elem. anal.;

DOI:10.1039/c1dt10372e

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