Technology Process of C28H37N5O8S
There total 6 articles about C28H37N5O8S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate;
In
1,2-dimethoxyethane; water;
at 85 ℃;
for 24h;
Combinatorial reaction / High throughput screening (HTS);
DOI:10.1021/co100060x
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; lithium hydroxide
2: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 25 °C
3: CuI immobilized on Amberlyst-21 / dichloromethane / 14 h / 20 °C / Combinatorial reaction / High throughput screening (HTS)
4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / 1,2-dimethoxyethane; water / 24 h / 85 °C / Combinatorial reaction / High throughput screening (HTS)
With
4-methyl-morpholine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
1,2-dimethoxyethane; dichloromethane; water;
3: Huisgen cycloaddition / 4: Suzuki coupling;
DOI:10.1021/co100060x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: CuI immobilized on Amberlyst-21 / dichloromethane / 14 h / 20 °C / Combinatorial reaction / High throughput screening (HTS)
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / 1,2-dimethoxyethane; water / 24 h / 85 °C / Combinatorial reaction / High throughput screening (HTS)
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate;
In
1,2-dimethoxyethane; dichloromethane; water;
1: Huisgen cycloaddition / 2: Suzuki coupling;
DOI:10.1021/co100060x