Technology Process of [(C12H4(CH3)4N2)((C6H5)3P)Cu(O2CH)]
There total 5 articles about [(C12H4(CH3)4N2)((C6H5)3P)Cu(O2CH)] which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
CO2; triphenyl phosphine;
In
ethanol;
byproducts: ethyl borate ester; bubbling CO2 through a soln. of 0.76mmol PPh3 in 10ml ethanol, addn. of0.19mmol Cu-complex, stirring for 2h while bubbling CO2 through the soln.; mechanism discussed;; evapn.; treatment of residue with diethyl ether, filtration, drying in vac.; elem. anal.;;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene
2: CO2; triphenyl phosphine / dichloromethane
3: ethanol
With
CO2; triphenyl phosphine;
In
ethanol; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene
2: CO2; triphenyl phosphine / dichloromethane
3: ethanol
With
CO2; triphenyl phosphine;
In
ethanol; dichloromethane; toluene;
