Technology Process of C54H59N3O11
There total 13 articles about C54H59N3O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at 0 - 20 ℃;
for 2h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1002/ejoc.201101815
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 0 - 20 °C
2: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / 0 °C
3: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
With
N-iodo-succinimide; copper(l) iodide; trimethylsilyl trifluoromethanesulfonate; water; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
DOI:10.1002/ejoc.201101815
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide / N,N-dimethyl-formamide / 4 h / 50 °C
2: copper(l) iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 0 - 20 °C
3: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / 0 °C
4: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
With
N-iodo-succinimide; copper(l) iodide; sodium azide; trimethylsilyl trifluoromethanesulfonate; water; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201101815
