C₂₁H₃₅NO₃Si

Base Information

Chemical Name:C₂₁H₃₅NO₃Si
CAS No.:1053703-07-3
Molecular Formula:C₂₁H₃₅NO₃Si
Molecular Weight:377.599
Hs Code.:

C<sub>21</sub>H<sub>35</sub>NO<sub>3</sub>Si

Synonyms:

Suppliers and Price of C₂₁H₃₅NO₃Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₁H₃₅NO₃Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₁H₃₅NO₃Si

There total 7 articles about C₂₁H₃₅NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 938449-12-8
(4S,5R,6S)-5-(tert-butyldimethylsilyloxy)-5,6-dihydro-4-isopropyl-2-phenyl-6-vinyl-4H-1,3-oxazine

: 1053703-07-3
C₂₁H₃₅NO₃Si

Guidance literature:: (4S,5R,6S)-5-(tert-butyldimethylsilyloxy)-5,6-dihydro-4-isopropyl-2-phenyl-6-vinyl-4H-1,3-oxazine; With hydrogenchloride; In tetrahydrofuran; methanol; at 20 ℃; for 12h;

With sodium hydrogencarbonate; In tetrahydrofuran; methanol; at 20 ℃; for 3h; pH=9.0; Further stages.;
DOI:10.1002/ejoc.200600927

Reference yield:

: 938448-94-3
(E)-3-[(4S,5S)-4,5-dihydro-4-isopropyl-2-phenyloxazol-5-yl]prop-2-en-1-ol

: 1053703-07-3
C₂₁H₃₅NO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 84 percent / p-toluenesulfonyl chloride; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / 20 °C

2.1: aq. HCl / tetrahydrofuran; methanol / 12 h / 20 °C

2.2: 97 percent / aq. sodium hydrogencarbonate / tetrahydrofuran; methanol / 3 h / 20 °C / pH 9.0

3.1: 94 percent / imidazole / dimethylformamide / 2 h / 20 °C

4.1: NaH; nBu₄NI; Pd(PPh₃)4 / tetrahydrofuran / 12 h / 40 °C

5.1: aq. HCl / tetrahydrofuran; methanol / 12 h / 20 °C

5.2: aq. sodium hydrogencarbonate / tetrahydrofuran; methanol / 3 h / 20 °C / pH 9.0

With 1H-imidazole; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra-(n-butyl)ammonium iodide; sodium hydride; p-toluenesulfonyl chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600927

Reference yield:

: 938448-98-7
(4S,5S)-5-[(E)-3-chloroprop-1-enyl]-4,5-dihydro-4-isopropyl-2-phenyloxazole

: 1053703-07-3
C₂₁H₃₅NO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: aq. HCl / tetrahydrofuran; methanol / 12 h / 20 °C

1.2: 97 percent / aq. sodium hydrogencarbonate / tetrahydrofuran; methanol / 3 h / 20 °C / pH 9.0

2.1: 94 percent / imidazole / dimethylformamide / 2 h / 20 °C

3.1: NaH; nBu₄NI; Pd(PPh₃)4 / tetrahydrofuran / 12 h / 40 °C

4.1: aq. HCl / tetrahydrofuran; methanol / 12 h / 20 °C

4.2: aq. sodium hydrogencarbonate / tetrahydrofuran; methanol / 3 h / 20 °C / pH 9.0

With 1H-imidazole; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600927