d4-1-methyl-4-phenyl-3-(5,6,7,8-tetraphenylnaphthalen-1-yl)isoquinoline

Base Information

• Chemical Name: d4-1-methyl-4-phenyl-3-(5,6,7,8-tetraphenylnaphthalen-1-yl)isoquinoline
• CAS No.: 1648787-50-1
• Molecular Formula: C₅₀H₃₅N
• Molecular Weight: 653.803
• Mol file: 1648787-50-1.mol

Synonyms:

Chemical Property of d4-1-methyl-4-phenyl-3-(5,6,7,8-tetraphenylnaphthalen-1-yl)isoquinoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of d4-1-methyl-4-phenyl-3-(5,6,7,8-tetraphenylnaphthalen-1-yl)isoquinoline

There total 1 articles about d4-1-methyl-4-phenyl-3-(5,6,7,8-tetraphenylnaphthalen-1-yl)isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

O-methyl acetophenone oxime (3376-33-8) + d5-acetophenone O-methyloxime (1352619-55-6) + diphenyl acetylene (501-65-5) → 1-methyl-4-phenyl-3-(5,6,7,8-tetraphenylnaphthalen-1-yl)isoquinoline (1648787-34-1) + d4-1-methyl-4-phenyl-3-(5,6,7,8-tetraphenylnaphthalen-1-yl)isoquinoline (1648787-50-1)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; sodium acetate; In methanol; at 110 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

DOI:10.1002/adsc.201400292

upstream raw materials:

O-methyl acetophenone oxime

d₅-acetophenone O-methyloxime

diphenyl acetylene