OsH₄(P(p-tolyl-o-d2)3)3

Base Information

• Chemical Name: OsH₄(P(p-tolyl-o-d2)3)3
• CAS No.: 133400-42-7
• Molecular Formula: C₆₃H₆₇OsP₃
• Molecular Weight: 1125.2

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Chemical Property of OsH₄(P(p-tolyl-o-d2)3)3

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Technology Process of OsH₄(P(p-tolyl-o-d2)3)3

There total 1 articles about OsH₄(P(p-tolyl-o-d2)3)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

OsD4(P(p-tolyl-o-d2)3)3 → OsH4(P(p-tolyl-o-d2)3)3 (133400-42-7) + OsHD3(P(p-tolyl-o-d2)3)3 + OsDH3(P(p-tolyl-o-d2)3)3 + OsH2D2(P(p-tolyl-o-d2)3)3

Guidance literature:

With hydrogen; In benzene; inert atmosphere of N2 or Ar; soln. degassed, stirred under 1 atm of hydrogen at room temp., flask sealed and heated at 75 ° C for 4 h; evapn., white powder, 0.17/0.48/0.32/0.02 mixture of mono,di-,tri-, tetrahydride by integration of the hydride resonance in the (1)H NMR spectrum, integration of the meta an d ortho resonances showed greater 92% d-atom in the ortho position;

DOI:10.1021/ja00011a019

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