C₃₁H₃₈F₆N₂O₃S

Base Information

• Chemical Name: C₃₁H₃₈F₆N₂O₃S
• CAS No.: 1399842-37-5
• Molecular Formula: C₃₁H₃₈F₆N₂O₃S
• Molecular Weight: 632.711
• Mol file: 1399842-37-5.mol

Synonyms:

Chemical Property of C₃₁H₃₈F₆N₂O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₈F₆N₂O₃S

There total 2 articles about C₃₁H₃₈F₆N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isosteviol (27975-19-5) → C31H38F6N2O3S (1399842-37-5)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium hydroxide / dimethyl sulfoxide / 3 h / 20 °C

2: selenium(IV) oxide; acetic anhydride / 6 h / Reflux

3: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol / Reflux

4: hydrogen / tetrahydrofuran / 5 h / 2585.81 Torr

5: dichloromethane / 2 h / 20 °C

With selenium(IV) oxide; hydroxylamine hydrochloride; hydrogen; acetic anhydride; sodium hydrogencarbonate; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;

DOI:10.1016/j.bmcl.2012.07.083

Reference yield:

C22H33BrO3 (1399842-41-1) → C31H38F6N2O3S (1399842-37-5)

Guidance literature:

Multi-step reaction with 4 steps

1: air / dimethyl sulfoxide / 16 h / Reflux

2: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol / Reflux

3: hydrogen / tetrahydrofuran / 5 h / 2585.81 Torr

4: dichloromethane / 2 h / 20 °C

With hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;

DOI:10.1016/j.bmcl.2012.07.083

Reference yield:

C31H38F6N2O3S (1399842-37-5) → C31H40F6N2O3S (1399842-50-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃; Reflux;

DOI:10.1016/j.bmcl.2012.07.083

upstream raw materials:

isosteviol

C₂₂H₃₃BrO₃

Downstream raw materials:

C₃₁H₄₀F₆N₂O₃S