Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N,N-dimethyl-

Base Information

Chemical Name:Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N,N-dimethyl-
CAS No.:137521-70-1
Molecular Formula:C10H6F15NO
Molecular Weight:
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N,N-dimethyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N,N-dimethyl-

There total 5 articles about Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 507-63-1
1-iodoheptadecafluorooctane

: 137521-70-1
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanoic acid dimethylamide

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / NH₃ / 0.67 h / Irradiation

2: 1.) NaH / 1.) ether, r.t., 30 min, 2.) ether

3: CHCl₃ / 2 h / 50 °C

4: NBS, PPHF / CH₂Cl₂ / 1 h / Ambient temperature

5: SiO₂

With N-Bromosuccinimide; ammonia; silica gel; sodium hydride; In dichloromethane; chloroform;
DOI:10.1055/s-1998-1913

Reference yield:

: 218163-04-3
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanethioic acid O-methyl ester

: 137521-70-1
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanoic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 2 h / 50 °C

2: NBS, PPHF / CH₂Cl₂ / 1 h / Ambient temperature

3: SiO₂

With N-Bromosuccinimide; silica gel; In dichloromethane; chloroform;
DOI:10.1055/s-1998-1913

Reference yield:

: 218163-06-5
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanethioic acid dimethylamide

: 137521-70-1
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanoic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: NBS, PPHF / CH₂Cl₂ / 1 h / Ambient temperature

2: SiO₂

With N-Bromosuccinimide; silica gel; In dichloromethane;
DOI:10.1055/s-1998-1913