2-fluorobenzyl-triethylphosphonium bromide

Base Information

Chemical Name:2-fluorobenzyl-triethylphosphonium bromide
CAS No.:1238861-70-5
Molecular Formula:Br*C₁₃H₂₁FP
Molecular Weight:307.186
Hs Code.:

Synonyms:

Suppliers and Price of 2-fluorobenzyl-triethylphosphonium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-fluorobenzyl-triethylphosphonium bromide

Chemical Property:

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Technology Process of 2-fluorobenzyl-triethylphosphonium bromide

There total 1 articles about 2-fluorobenzyl-triethylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: triethylphosphane hydrochloride

: 446-51-5
2-fluorobenzyl alcohol

: 1238861-70-5
2-fluorobenzyl-triethylphosphonium bromide

Guidance literature:: at 100 ℃; for 8h; Microwave irradiation; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.08.040

Reference yield:

: 1238861-70-5
2-fluorobenzyl-triethylphosphonium bromide

: 1335205-41-8
Br^(1-)*C₂₇H₃₉FP⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide / water / 0.05 h / Inert atmosphere

1.2: 3 h / 80 °C / Inert atmosphere

2.1: 0.5 h / 160 °C / Inert atmosphere; Microwave irradiation

With lithium hydroxide; In water; 1.2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.08.040

Reference yield:

: 1238861-70-5
2-fluorobenzyl-triethylphosphonium bromide

: 1335205-45-2
C₂₂H₁₅F₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hydroxide / water / 0.05 h / Inert atmosphere

1.2: 3 h / 80 °C / Inert atmosphere

2.1: 0.5 h / 160 °C / Inert atmosphere; Microwave irradiation

3.1: lithium hydroxide / water / 0.05 h / Inert atmosphere

3.2: 5 h / 80 °C / Inert atmosphere

With lithium hydroxide; In water; 1.2: Wittig reaction / 3.2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.08.040