Ac-T(4-SO₂Me-Phe)PN-NH₂

Base Information

Chemical Name:Ac-T(4-SO₂Me-Phe)PN-NH₂
CAS No.:1354454-17-3
Molecular Formula:C₂₅H₃₆N₆O₉S
Molecular Weight:596.662
Hs Code.:

Ac-T(4-SO<sub>2</sub>Me-Phe)PN-NH<sub>2</sub>

Synonyms:

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Chemical Property of Ac-T(4-SO₂Me-Phe)PN-NH₂

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Technology Process of Ac-T(4-SO₂Me-Phe)PN-NH₂

There total 3 articles about Ac-T(4-SO₂Me-Phe)PN-NH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Ac-T(4-I-Phe)PN-NH₂

: 1354454-17-3
Ac-T(4-SO₂Me-Phe)PN-NH₂

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; 1,10-Phenanthroline; N-ethyl-N,N-diisopropylamine / tert-Amyl alcohol / 11 h / 90 °C

2: DL-dithiothreitol / 1 h / 20 °C / pH 7.2 / aq. phosphate buffer

3: 1 h / 20 °C / pH 8 / aq. phosphate buffer

4: formic acid; dihydrogen peroxide / water / 2 h / 20 °C

With copper(l) iodide; formic acid; 1,10-Phenanthroline; DL-dithiothreitol; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; In tert-Amyl alcohol; water;
DOI:10.1021/ol202947f

Reference yield:

: 1354453-80-7
Ac-T(4-SH-Phe)PN-NH₂

: 1354454-17-3
Ac-T(4-SO₂Me-Phe)PN-NH₂

Guidance literature:: Multi-step reaction with 2 steps

1: 1 h / 20 °C / pH 8 / aq. phosphate buffer

2: formic acid; dihydrogen peroxide / water / 2 h / 20 °C

With formic acid; dihydrogen peroxide; In water;
DOI:10.1021/ol202947f

Reference yield:

: 1354453-75-0
Ac-T(4-thioacetyl-Phe)PN-NH₂

: 1354454-17-3
Ac-T(4-SO₂Me-Phe)PN-NH₂

Guidance literature:: Multi-step reaction with 3 steps

1: DL-dithiothreitol / 1 h / 20 °C / pH 7.2 / aq. phosphate buffer

2: 1 h / 20 °C / pH 8 / aq. phosphate buffer

3: formic acid; dihydrogen peroxide / water / 2 h / 20 °C

With formic acid; DL-dithiothreitol; dihydrogen peroxide; In water;
DOI:10.1021/ol202947f