Technology Process of C19H17NO4S
There total 4 articles about C19H17NO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen; acetic acid;
under 9120.61 Torr;
DOI:10.1691/ph.2010.9706
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / 0.5 h / 20 °C / Inert atmosphere
1.2: 21 h / 20 - 100 °C
2.1: sodium acetate / 0.17 h / 110 °C / Microwave irradiation
3.1: palladium 10% on activated carbon; hydrogen; acetic acid / 9120.61 Torr
With
bis-triphenylphosphine-palladium(II) chloride; palladium 10% on activated carbon; hydrogen; sodium acetate; acetic acid; triethylamine;
1.1: Sonogashira coupling / 1.2: Sonogashira coupling;
DOI:10.1691/ph.2010.9706
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / 0.5 h / 20 °C / Inert atmosphere
1.2: 21 h / 20 - 100 °C
2.1: sodium acetate / 0.17 h / 110 °C / Microwave irradiation
3.1: palladium 10% on activated carbon; hydrogen; acetic acid / 9120.61 Torr
With
bis-triphenylphosphine-palladium(II) chloride; palladium 10% on activated carbon; hydrogen; sodium acetate; acetic acid; triethylamine;
1.1: Sonogashira coupling / 1.2: Sonogashira coupling;
DOI:10.1691/ph.2010.9706