C₅₆H₇₀F₉N₆O₁₅S₂⁽¹⁺⁾

Base Information

Chemical Name:C₅₆H₇₀F₉N₆O₁₅S₂⁽¹⁺⁾
CAS No.:1643531-31-0
Molecular Formula:C₅₆H₇₀F₉N₆O₁₅S₂
Molecular Weight:1302.32
Hs Code.:

C<sub>56</sub>H<sub>70</sub>F<sub>9</sub>N<sub>6</sub>O<sub>15</sub>S<sub>2</sub><sup>(1+)</sup>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₆H₇₀F₉N₆O₁₅S₂⁽¹⁺⁾

Chemical Property:

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Technology Process of C₅₆H₇₀F₉N₆O₁₅S₂⁽¹⁺⁾

There total 8 articles about C₅₆H₇₀F₉N₆O₁₅S₂⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₂H₆₇F₉N₅O₁₃S₂⁽¹⁺⁾

: 105832-38-0
O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

: 1643531-31-0
C₅₆H₇₀F₉N₆O₁₅S₂⁽¹⁺⁾

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1039/c4ob00456f

Reference yield:

: 1643531-20-7
C₃₅H₃₄F₉N₂O₅⁽¹⁺⁾

: 1643531-31-0
C₅₆H₇₀F₉N₆O₁₅S₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,6-di-tert-butyl-pyridine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate / 16 h / 155 °C / Sealed tube

2.1: hydrogenchloride / acetonitrile / 16 h / Reflux

3.1: O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C / Cooling with ice

3.2: 2 h / 0 °C

4.1: N-ethyl-N,N-diisopropylamine / methanol / 1 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

With hydrogenchloride; 2,6-di-tert-butyl-pyridine; O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c4ob00456f

Reference yield:

: 3179-63-3
3-Dimethylamino-1-propanol

: 1643531-31-0
C₅₆H₇₀F₉N₆O₁₅S₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 7 steps

2.1: potassium carbonate / acetonitrile / 1 h / 20 °C

3.1: 2,6-di-tert-butyl-pyridine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate / 16 h / 155 °C / Sealed tube

4.1: hydrogenchloride / acetonitrile / 16 h / Reflux

5.1: O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C / Cooling with ice

5.2: 2 h / 0 °C

6.1: N-ethyl-N,N-diisopropylamine / methanol / 1 h / 20 °C

7.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

With hydrogenchloride; 2,6-di-tert-butyl-pyridine; potassium carbonate; O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; In methanol; N,N-dimethyl-formamide; acetonitrile; 1.1: |Mitsunobu Displacement;
DOI:10.1039/c4ob00456f