tris(trimethylsilyl)silylphenylacetylene dicobalt hexacarbonyl

Base Information

• Chemical Name: tris(trimethylsilyl)silylphenylacetylene dicobalt hexacarbonyl
• CAS No.: 912560-63-5
• Molecular Formula: C₂₃H₃₂Co₂O₆Si₄
• Molecular Weight: 634.832

Synonyms:

Chemical Property of tris(trimethylsilyl)silylphenylacetylene dicobalt hexacarbonyl

Chemical Property:

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Technology Process of tris(trimethylsilyl)silylphenylacetylene dicobalt hexacarbonyl

There total 1 articles about tris(trimethylsilyl)silylphenylacetylene dicobalt hexacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

dicobalt octacarbonyl (15226-74-1,61091-28-9,61117-58-6) + tris(trimethylsilyl)silylphenylacetylene → tris(trimethylsilyl)silylphenylacetylene dicobalt hexacarbonyl (912560-63-5)

Guidance literature:

In pentane; (N2); Schlenk technique; soln. of alkynyl silane in pentane was added dropwise to soln. of Co complex (1 equiv.) in pentane at room temp.; soln.was stirred for 12 h; solvent reduced (vac.); recrystd. (-70°C); elem. anal.;

DOI:10.1021/om0604831

upstream raw materials:

dicobalt octacarbonyl

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