PhC(NtBu)2-chlorosilylene 9-borabicyclo[3.3.1]nonane adduct

Base Information

Chemical Name:PhC(NtBu)2-chlorosilylene 9-borabicyclo[3.3.1]nonane adduct
CAS No.:1353018-19-5
Molecular Formula:C₂₃H₃₈BClN₂Si
Molecular Weight:416.918
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Chemical Property of PhC(NtBu)2-chlorosilylene 9-borabicyclo[3.3.1]nonane adduct

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Technology Process of PhC(NtBu)2-chlorosilylene 9-borabicyclo[3.3.1]nonane adduct

There total 1 articles about PhC(NtBu)2-chlorosilylene 9-borabicyclo[3.3.1]nonane adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.6%

: N,N′-di-tertbutyl(phenylamidinato)chlorosilylene

: 280-64-8
9-bora-bicyclo[3.3.1]nonane

: 1353018-19-5
PhC(NtBu)2-chlorosilylene 9-borabicyclo[3.3.1]nonane adduct

Guidance literature:: In tetrahydrofuran; toluene; Schlenk technique, N2; to chlorosilylene soln. in toluene, 9-BBN soln. in THF added at -78°C, stirred and warmed to room temp., then stirring for 12 h; soln. filtered, solvent removed in vac., stored (-32°C, 14 h); elem. anal.;
DOI:10.1002/ejic.201100661