Technology Process of C13H18N4O
There total 8 articles about C13H18N4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / tetrahydrofuran; mineral oil / 15 h / 20 °C
2: sodium azide; ammonium chloride / water; acetone / 15 h / Reflux
With
sodium azide; sodium hydride; ammonium chloride;
In
tetrahydrofuran; water; acetone; mineral oil;
DOI:10.1055/s-0033-1340250
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dichloromethane / 0.17 h / 20 °C
1.2: 15 h / Reflux
2.1: sodium hydride / tetrahydrofuran; mineral oil / 15 h / 20 °C
3.1: sodium azide; ammonium chloride / water; acetone / 15 h / Reflux
With
sodium azide; sodium hydride; ammonium chloride;
In
tetrahydrofuran; dichloromethane; water; acetone; mineral oil;
DOI:10.1055/s-0033-1340250
- Guidance literature:
-
With
sodium azide; ammonium chloride;
In
water; acetone;
for 15h;
Reflux;
DOI:10.1055/s-0033-1340250