Technology Process of (Z)-8-phenyloct-5-en-2-one
There total 5 articles about (Z)-8-phenyloct-5-en-2-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrosulfite; sodium hydrogencarbonate;
In
ethanol; water;
for 4h;
Reflux;
Inert atmosphere;
DOI:10.1021/ja207944c
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.33 h / Inert atmosphere
1.2: Inert atmosphere
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
3.1: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux
4.1: sodium hydrosulfite; sodium hydrogencarbonate / ethanol; water / 4 h / Reflux; Inert atmosphere
With
sodium hydrosulfite; dilauryl peroxide; sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; mineral oil;
DOI:10.1021/ja207944c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
2: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux
3: sodium hydrosulfite; sodium hydrogencarbonate / ethanol; water / 4 h / Reflux; Inert atmosphere
With
sodium hydrosulfite; dilauryl peroxide; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/ja207944c
