C₂₇H₂₄BF₄N₇

Base Information

• Chemical Name: C₂₇H₂₄BF₄N₇
• CAS No.: 1616353-76-4
• Molecular Formula: C₂₇H₂₄BF₄N₇
• Molecular Weight: 533.339
• Mol file: 1616353-76-4.mol

Synonyms:

Chemical Property of C₂₇H₂₄BF₄N₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₇H₂₄BF₄N₇

There total 2 articles about C₂₇H₂₄BF₄N₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Pentyne (627-19-0) + C15H9BCl2F2N3Pol + 3,5-difluorobenzylamine (90390-27-5) → C27H24BF4N7 (1616353-76-4)

Guidance literature:

C₁₅H₉BCl₂F₂N₃Pol; With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; 2-chlorotrityl chloride polystyrene resin

3,5-difluorobenzylamine; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1h; 2-chlorotrityl chloride polystyrene resin

1-Pentyne; Further stages;

DOI:10.1039/c6cc00095a

Reference yield:

→ C27H24BF4N7 (1616353-76-4)

Guidance literature:

With 2-chlorotrityl chloride polystyrene resin; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 24h;

With sodium azide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Further stages;

upstream raw materials:

1-Pentyne

3,5-difluorobenzylamine