C₄₁H₄₂O₁₂

Base Information

• Chemical Name: C₄₁H₄₂O₁₂
• CAS No.: 1315568-03-6
• Molecular Formula: C₄₁H₄₂O₁₂
• Molecular Weight: 726.777
• Mol file: 1315568-03-6.mol

Synonyms:

Chemical Property of C₄₁H₄₂O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₄₂O₁₂

There total 12 articles about C₄₁H₄₂O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C41H44O12 (1315567-75-9) → C41H42O12 (1315568-03-6)

Guidance literature:

With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃;

DOI:10.1038/nchem.1074

Reference yield:

C24H28O7 → C41H42O12 (1315568-03-6)

Guidance literature:

Multi-step reaction with 10 steps

1.1: 122 °C / neat (no solvent)

1.2: 20 °C

2.1: 1,2-dichloro-benzene / 250 °C / Microwave irradiation

3.1: iodine; magnesium / diethyl ether / 0 °C

4.1: pyridine; dibromo sulfoxide / diethyl ether / -40 °C

5.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 °C

6.1: methyllithium lithium bromide / tetrahydrofuran / -78 - 20 °C

7.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; formic acid / toluene / 20 °C

8.1: ozone / methanol; dichloromethane / -78 °C

8.2: -78 - 20 °C

9.1: 1H-imidazole; tert-butyldimethylsilyl chloride / dichloromethane / 20 °C

9.2: 20 °C

10.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

With pyridine; 1H-imidazole; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; dibromo sulfoxide; formic acid; methyllithium lithium bromide; tetrabutyl ammonium fluoride; iodine; sodium hydrogencarbonate; Dess-Martin periodane; ozone; magnesium; tert-butyldimethylsilyl chloride; acetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 1,2-dichloro-benzene; toluene; 1.1: Claisen rearrangement;

DOI:10.1038/nchem.1074

Reference yield:

C41H55BrO6Si → C41H42O12 (1315568-03-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ozone / methanol; dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: 1H-imidazole; tert-butyldimethylsilyl chloride / dichloromethane / 20 °C

2.2: 20 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

With 1H-imidazole; sodium hydrogencarbonate; Dess-Martin periodane; ozone; tert-butyldimethylsilyl chloride; In methanol; dichloromethane;

DOI:10.1038/nchem.1074

upstream raw materials:

C₃₃H₅₂O₉Si

C₄₁H₄₄O₁₂

C₃₃H₄₇BrO₆Si

C₃₆H₅₆O₇Si₂

Downstream raw materials:

C₄₄H₄₈O₁₂

C₄₃H₅₈O₁₀Si

C₄₅H₅₈O₁₀Si

C₄₃H₅₆O₉Si

Refernces