(5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid

Base Information

Chemical Name:(5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid
CAS No.:116227-11-3
Molecular Formula:C₂₂H₂₁N₅O₈
Molecular Weight:483.437
Hs Code.:

(5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid

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Chemical Property of (5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid

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Technology Process of (5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid

There total 6 articles about (5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

: 116227-11-3
(5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid

Guidance literature:: With trifluoroacetic acid; In various solvent(s); for 0.166667h; Ambient temperature;
DOI:10.1248/cpb.36.1309

Reference yield:

: 17376-04-4
2-phenethyl iodide

: 116227-11-3
(5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide

2: ammonia / methanol / 1 h

3: trifluoroacetic acid / various solvent(s) / 0.17 h / Ambient temperature

With ammonia; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.1309

Reference yield:

: 98871-07-9
dibenzhydryl griseolate

: 116227-11-3
(5R,6R)-2-(Carboxy-hydroxy-methyl)-6-hydroxy-5-(6-imino-1-phenethyl-1,6-dihydro-purin-9-yl)-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 3 h / Ambient temperature

2: dimethylformamide

3: ammonia / methanol / 1 h

4: trifluoroacetic acid / various solvent(s) / 0.17 h / Ambient temperature

With pyridine; ammonia; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.1309