trans-N-(4-methylphenyl)sulfonyl-2-(2-buten-1-yloxy)aniline

Base Information

Chemical Name:trans-N-(4-methylphenyl)sulfonyl-2-(2-buten-1-yloxy)aniline
CAS No.:1361843-81-3
Molecular Formula:C₁₇H₁₉NO₃S
Molecular Weight:317.409
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-N-(4-methylphenyl)sulfonyl-2-(2-buten-1-yloxy)aniline

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Technology Process of trans-N-(4-methylphenyl)sulfonyl-2-(2-buten-1-yloxy)aniline

There total 1 articles about trans-N-(4-methylphenyl)sulfonyl-2-(2-buten-1-yloxy)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107616-15-9,132396-65-7
2-(3-methylallyloxy)aniline

: 98-59-9
p-toluenesulfonyl chloride

: (Z)-N-(2-(but-2-en-1-yloxy)phenyl)-4-methylbenzenesulfonamide

: 1361843-81-3
trans-N-(4-methylphenyl)sulfonyl-2-(2-buten-1-yloxy)aniline

Guidance literature:: With pyridine; In dichloromethane;
DOI:10.1021/ol300030w

Reference yield:

: 1361843-81-3
trans-N-(4-methylphenyl)sulfonyl-2-(2-buten-1-yloxy)aniline

: 4-tosyl-3-vinyl-3,4-dihydro-2H-benzo[b][1,4]oxazine

: 4-tosyl-3-vinyl-3,4-dihydro-2H-benzo[b][1,4]oxazine

Guidance literature:: With (P,R,R)-i-Pr-SPRIX; oxone||potassium monopersulfate triple salt; palladium diacetate; In chlorobenzene; at 60 ℃; for 27h; Reagent/catalyst; Solvent; Overall yield = 88 %; Overall yield = 0.44 g; enantioselective reaction; Catalytic behavior; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.8b02946