C₅₇H₆₂NO₁₅S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₅₇H₆₂NO₁₅S^(1-)*Na⁽¹⁺⁾
CAS No.:1380244-30-3
Molecular Formula:C₅₇H₆₂NO₁₅S*Na
Molecular Weight:1056.17
Hs Code.:

C<sub>57</sub>H<sub>62</sub>NO<sub>15</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

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Chemical Property of C₅₇H₆₂NO₁₅S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₅₇H₆₂NO₁₅S^(1-)*Na⁽¹⁺⁾

There total 7 articles about C₅₇H₆₂NO₁₅S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1380244-29-0
C₅₇H₆₃NO₁₂

: 1380244-30-3
C₅₇H₆₂NO₁₅S^(1-)*Na⁽¹⁺⁾

Guidance literature:: With pyridine; sulfur trioxide pyridine complex; at 65 ℃; for 1.5h;
DOI:10.1016/j.carres.2012.03.033

Reference yield:

: C₅₇H₆₁NO₁₂

: 1380244-30-3
C₅₇H₆₂NO₁₅S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / -78 °C / Molecular sieve

2: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / -60 - -30 °C

3: potassium tri-sec-butyl-borohydride / -78 - -30 °C

4: pyridine; sulfur trioxide pyridine complex / 1.5 h / 65 °C

With pyridine; triethylsilane; oxalyl dichloride; trifluorormethanesulfonic acid; sulfur trioxide pyridine complex; potassium tri-sec-butyl-borohydride; triethylamine; In dichloromethane; dimethyl sulfoxide; 2: Swern oxidation;
DOI:10.1016/j.carres.2012.03.033

Reference yield:

: 1380244-28-9
C₅₇H₆₃NO₁₂

: 1380244-30-3
C₅₇H₆₂NO₁₅S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / -60 - -30 °C

2: potassium tri-sec-butyl-borohydride / -78 - -30 °C

3: pyridine; sulfur trioxide pyridine complex / 1.5 h / 65 °C

With pyridine; oxalyl dichloride; sulfur trioxide pyridine complex; potassium tri-sec-butyl-borohydride; triethylamine; In dichloromethane; dimethyl sulfoxide; 1: Swern oxidation;
DOI:10.1016/j.carres.2012.03.033