C₂₂H₂₉BrN₂O₈

Base Information

Chemical Name:C₂₂H₂₉BrN₂O₈
CAS No.:1357623-17-6
Molecular Formula:C₂₂H₂₉BrN₂O₈
Molecular Weight:529.385
Hs Code.:

C<sub>22</sub>H<sub>29</sub>BrN<sub>2</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₂₂H₂₉BrN₂O₈

Chemical Property:

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Technology Process of C₂₂H₂₉BrN₂O₈

There total 21 articles about C₂₂H₂₉BrN₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55904-12-6
((4R,5S)-5-Hydroxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methanol

: 1357623-17-6
C₂₂H₂₉BrN₂O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: amano Porcine pancreas lipase / 20 h / 20 °C / Inert atmosphere; Enzymatic reaction

2.1: triethylamine / dichloromethane / -18 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 42 h / 100 °C / Inert atmosphere

4.1: potassium hydroxide / methanol / 0.33 h / 0 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.17 h / -70 °C / Inert atmosphere

5.2: 1 h / -70 - -60 °C / Inert atmosphere

6.1: triphenylphosphine / tetrahydrofuran / 24 h / 50 °C / Inert atmosphere; Molecular sieve

7.1: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

8.1: hydrogen fluoride / water; acetonitrile / -10 °C

9.1: Jones reagent / acetone / 1.2 h / 0 °C

10.1: tetrahydrofuran / 0 °C / Inert atmosphere

With Jones reagent; sodium azide; oxalyl dichloride; amano Porcine pancreas lipase; hydrogen fluoride; dimethyl sulfoxide; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; 5.1: Swern oxidation / 5.2: Swern oxidation / 7.1: Ugi condensation;
DOI:10.1039/c1ob06632c

Reference yield:

: 1357623-31-4
C₇H₁₁N₃O₃

: 1357623-17-6
C₂₂H₂₉BrN₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine / tetrahydrofuran / 24 h / 50 °C / Inert atmosphere; Molecular sieve

2: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

3: hydrogen fluoride / water; acetonitrile / -10 °C

4: Jones reagent / acetone / 1.2 h / 0 °C

5: tetrahydrofuran / 0 °C / Inert atmosphere

With Jones reagent; hydrogen fluoride; triphenylphosphine; In tetrahydrofuran; methanol; water; acetone; acetonitrile; 2: Ugi condensation;
DOI:10.1039/c1ob06632c

Reference yield:

: C₁₀H₁₈O₇S

: 1357623-17-6
C₂₂H₂₉BrN₂O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium azide / N,N-dimethyl-formamide / 42 h / 100 °C / Inert atmosphere

2.1: potassium hydroxide / methanol / 0.33 h / 0 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.17 h / -70 °C / Inert atmosphere

3.2: 1 h / -70 - -60 °C / Inert atmosphere

4.1: triphenylphosphine / tetrahydrofuran / 24 h / 50 °C / Inert atmosphere; Molecular sieve

5.1: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: hydrogen fluoride / water; acetonitrile / -10 °C

7.1: Jones reagent / acetone / 1.2 h / 0 °C

8.1: tetrahydrofuran / 0 °C / Inert atmosphere

With Jones reagent; sodium azide; oxalyl dichloride; hydrogen fluoride; dimethyl sulfoxide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; 3.1: Swern oxidation / 3.2: Swern oxidation / 5.1: Ugi condensation;
DOI:10.1039/c1ob06632c