C₄₉H₈₈O₁₂Si₂

Base Information

Chemical Name:C₄₉H₈₈O₁₂Si₂
CAS No.:1431725-78-8
Molecular Formula:C₄₉H₈₈O₁₂Si₂
Molecular Weight:925.402
Hs Code.:

C<sub>49</sub>H<sub>88</sub>O<sub>12</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₄₉H₈₈O₁₂Si₂

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Technology Process of C₄₉H₈₈O₁₂Si₂

There total 25 articles about C₄₉H₈₈O₁₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431725-77-7
C₄₉H₈₆O₁₂Si₂

: 1431725-78-8
C₄₉H₈₈O₁₂Si₂

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; Inert atmosphere;
DOI:10.1002/anie.201203406

Reference yield:

: 1431725-87-9
C₁₅H₂₀O₅

: 1431725-78-8
C₄₉H₈₈O₁₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: chromium dichloride / tetrahydrofuran / 2.33 h / 0 - 20 °C

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / -78 - 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: water; methanesulfonamide; AD-mix-β / tert-butyl alcohol / 48 h / 0 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / Inert atmosphere

5.1: diisobutylaluminium hydride / dichloromethane; hexane / -78 °C / Inert atmosphere

With 1H-imidazole; chromium dichloride; methanesulfonamide; AD-mix-β; water; diisobutylaluminium hydride; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: |Takai-Utimoto Olefination / 2.2: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201203406

Reference yield:

: 168777-81-9
(3S,4R)-1-[(tert-butyldimethylsilyl)oxy]-4-methylhex-5-en-3-ol

: 1431725-78-8
C₄₉H₈₈O₁₂Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 0 °C / Inert atmosphere

2.1: camphorsulfonic acid / dichloromethane / 2.5 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; hexane / -78 - 0 °C / Inert atmosphere

4.1: Jones reagent / acetone

5.1: diethyl ether / 1 h / 0 °C

6.1: ozone / dichloromethane / -78 °C

7.1: chromium dichloride / tetrahydrofuran / 2.33 h / 0 - 20 °C

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / -78 - 20 °C / Inert atmosphere

8.2: Inert atmosphere

9.1: water; methanesulfonamide; AD-mix-β / tert-butyl alcohol / 48 h / 0 °C

10.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / Inert atmosphere

11.1: diisobutylaluminium hydride / dichloromethane; hexane / -78 °C / Inert atmosphere

With 1H-imidazole; chromium dichloride; Jones reagent; methanesulfonamide; AD-mix-β; water; diisobutylaluminium hydride; ozone; tetra-n-butylammoniumfluoride trihydrate; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; tert-butyl alcohol; 4.1: |Jones Oxidation / 7.1: |Takai-Utimoto Olefination / 8.2: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201203406