Spiro-2-methyl-1'-oxo-2'-benzyl

Base Information

Chemical Name:Spiro-2-methyl-1'-oxo-2'-benzyl
CAS No.:137660-62-9
Molecular Formula:C₂₂H₂₃NO
Molecular Weight:317.431
Hs Code.:

Spiro<cyclohex-3-ene-1,4'(3'H)-isoquinoleine>-2-methyl-1'-oxo-2'-benzyl

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Chemical Property of Spiro-2-methyl-1'-oxo-2'-benzyl

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Technology Process of Spiro-2-methyl-1'-oxo-2'-benzyl

There total 4 articles about Spiro-2-methyl-1'-oxo-2'-benzyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 137660-61-8
N-(2-Methylcyclohex-3-enylidene)-N-benzylbenzamide

: 137660-62-9,137765-18-5
Spiro-2-methyl-1'-oxo-2'-benzyl

Guidance literature:: In methanol; for 48h; Irradiation;
DOI:10.1016/S0040-4020(01)89731-3

Reference yield:

: 17775-58-5
3-methyl-4-formylcyclohexene

: 137660-62-9,137765-18-5
Spiro-2-methyl-1'-oxo-2'-benzyl

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / p-TsOH / benzene / 2 h / Heating

2: 30 percent / Et₃N / benzene / 15 h / Ambient temperature

3: 84 percent / methanol / 48 h / Irradiation

With toluene-4-sulfonic acid; triethylamine; In methanol; benzene;
DOI:10.1016/S0040-4020(01)89731-3

Reference yield:

: Benzyl-[2-methyl-cyclohex-3-en-(Z)-ylidenemethyl]-amine

: 137660-62-9,137765-18-5
Spiro-2-methyl-1'-oxo-2'-benzyl

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / Et₃N / benzene / 15 h / Ambient temperature

2: 84 percent / methanol / 48 h / Irradiation

With triethylamine; In methanol; benzene;
DOI:10.1016/S0040-4020(01)89731-3