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Technology Process of Co(NH3)5(OC6H4CO2CH3)(2+)*3Na(1+)*5ClO4(1-)=Co(NH3)5(OC6H4CO2CH3)(ClO4)2*3NaClO4

Co(NH3)5(OC6H4CO2CH3)(2+)*3Na(1+)*5ClO4(1-)=Co(NH3)5(OC6H4CO2CH3)(ClO4)2*3NaClO4

Base Information
  • Chemical Name:Co(NH3)5(OC6H4CO2CH3)(2+)*3Na(1+)*5ClO4(1-)=Co(NH3)5(OC6H4CO2CH3)(ClO4)2*3NaClO4
  • CAS No.:80679-86-3
  • Molecular Formula:C8H22CoN5O3*5ClO4*3Na
  • Molecular Weight:861.51
  • Hs Code.:
Co(NH<sub>3</sub>)5(OC<sub>6</sub>H<sub>4</sub>CO<sub>2</sub>CH<sub>3</sub>)<sup>(2+)</sup>*3Na<sup>(1+)</sup>*5ClO<sub>4</sub><sup>(1-)</sup>=Co(NH<sub>3</sub>)5(OC<sub>6</sub>H<sub>4</sub>CO<sub>2</sub>CH<sub>3</sub>)(ClO<sub>4</sub>)2*3NaClO<sub>4</sub>

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Chemical Property of Co(NH3)5(OC6H4CO2CH3)(2+)*3Na(1+)*5ClO4(1-)=Co(NH3)5(OC6H4CO2CH3)(ClO4)2*3NaClO4
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Technology Process of Co(NH3)5(OC6H4CO2CH3)(2+)*3Na(1+)*5ClO4(1-)=Co(NH3)5(OC6H4CO2CH3)(ClO4)2*3NaClO4

There total 1 articles about Co(NH3)5(OC6H4CO2CH3)(2+)*3Na(1+)*5ClO4(1-)=Co(NH3)5(OC6H4CO2CH3)(ClO4)2*3NaClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trifluoromethanesulfonatopentaamminecobalt(III) trifluoromethanesulfonate
115245-01-7

trifluoromethanesulfonatopentaamminecobalt(III) trifluoromethanesulfonate

methyl 4-hydroxylbenzoate
99-76-3,156291-94-0

methyl 4-hydroxylbenzoate

Co(NH<sub>3</sub>)5(OC<sub>6</sub>H<sub>4</sub>CO<sub>2</sub>CH<sub>3</sub>)<sup>(2+)</sup>*3Na<sup>(1+)</sup>*5ClO<sub>4</sub><sup>(1-)</sup>=Co(NH<sub>3</sub>)5(OC<sub>6</sub>H<sub>4</sub>CO<sub>2</sub>CH<sub>3</sub>)(ClO<sub>4</sub>)2*3NaClO<sub>4</sub>
80679-86-3

Co(NH3)5(OC6H4CO2CH3)(2+)*3Na(1+)*5ClO4(1-)=Co(NH3)5(OC6H4CO2CH3)(ClO4)2*3NaClO4

Guidance literature:
With 2,6-dimethylpyridine; sodium perchlorate; In sulfolane; Co complex reacting in sulfolane with 2,6-dimethylpyridine and the ester for 24 h, filtering, adding to 2-butanol in Et2O, solvent decanting off, purified on ion exchanged resin, treating with warm aq. NaClO4, cooling, ppt. washing with Et2O, air-drying; identified by elem. anal., IR, UV and NMR spectra;
DOI:10.1021/ic00135a074
upstream raw materials:

trifluoromethanesulfonatopentaamminecobalt(III) trifluoromethanesulfonate

methyl 4-hydroxylbenzoate

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