Technology Process of C28H37N3O10S
There total 4 articles about C28H37N3O10S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C
2: 20% palladium hydroxide-activated charcoal; hydrogen / methanol; ethyl acetate / 6 h / 20 °C
3: 4-methyl-morpholine / N,N-dimethyl-formamide / 20 °C
With
4-methyl-morpholine; di-isopropyl azodicarboxylate; 20% palladium hydroxide-activated charcoal; hydrogen; triphenylphosphine;
In
tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide;
1: |Mitsunobu Displacement;
DOI:10.1002/chem.201203794
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 20% palladium hydroxide-activated charcoal; hydrogen / methanol; ethyl acetate / 6 h / 20 °C
2: 4-methyl-morpholine / N,N-dimethyl-formamide / 20 °C
With
4-methyl-morpholine; 20% palladium hydroxide-activated charcoal; hydrogen;
In
methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/chem.201203794