C₃₀H₃₃NO₃

Base Information

Chemical Name:C₃₀H₃₃NO₃
CAS No.:1447825-77-5
Molecular Formula:C₃₀H₃₃NO₃
Molecular Weight:455.597
Hs Code.:

C<sub>30</sub>H<sub>33</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₃₀H₃₃NO₃

Chemical Property:

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Technology Process of C₃₀H₃₃NO₃

There total 11 articles about C₃₀H₃₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₃NO

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1447825-77-5
C₃₀H₃₃NO₃

Guidance literature:: With sodium carbonate; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1021/jm400542h

Reference yield:

: 251444-03-8
(1R,2S)-2-(tert-butyldiphenylsilyloxy)methyl-1-formylcyclopropane

: 1447825-77-5
C₃₀H₃₃NO₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C

1.2: 0.33 h / 0 °C

2.1: water; hydrogenchloride / tetrahydrofuran / 1 h / 0 °C

3.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tert-butyl alcohol; water / 0.67 h / 20 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

5.2: 1 h / -78 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

6.2: 24 h / -78 °C

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.33 h / -78 °C

7.2: 1 h / 20 °C

8.1: copper(II) sulfate / dichloromethane / 22 h / 20 °C

9.1: tetrahydrofuran; dichloromethane / 0.67 h / 20 °C

10.1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

11.1: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

With hydrogenchloride; sodium chlorite; n-butyllithium; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; water; sodium hexamethyldisilazane; diisobutylaluminium hydride; sodium carbonate; copper(II) sulfate; triethylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol; 1.1: |Wittig Olefination / 9.1: |Grignard Reaction;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-68-4
C₃₃H₃₉NO₄Si

: 1447825-77-5
C₃₀H₃₃NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.33 h / -78 °C

1.2: 1 h / 20 °C

2.1: copper(II) sulfate / dichloromethane / 22 h / 20 °C

3.1: tetrahydrofuran; dichloromethane / 0.67 h / 20 °C

4.1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

5.1: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

With hydrogenchloride; diisobutylaluminium hydride; sodium carbonate; copper(II) sulfate; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; 3.1: |Grignard Reaction;
DOI:10.1021/jm400542h