Technology Process of C42H51BF2N2O10
There total 8 articles about C42H51BF2N2O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium iodide;
In
ethyl acetate;
for 16h;
Reflux;
Inert atmosphere;
DOI:10.1002/chem.201303868
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / dichloromethane; methanol / 5 h / 20 °C / 760.05 Torr
3: dicyclohexyl-carbodiimide / diethyl ether / 5 h / 20 °C
4: piperidine; acetic acid / toluene / 12 h / Dean-Stark; Reflux
5: hydrogenchloride / nitromethane / 4 h / 0 - 20 °C
With
piperidine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; dicyclohexyl-carbodiimide;
In
methanol; diethyl ether; nitromethane; dichloromethane; toluene;
4: |Knoevenagel Condensation;
DOI:10.1002/chem.201303868
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dicyclohexyl-carbodiimide / diethyl ether / 5 h / 20 °C
2: piperidine; acetic acid / toluene / 12 h / Dean-Stark; Reflux
3: hydrogenchloride / nitromethane / 4 h / 0 - 20 °C
With
piperidine; hydrogenchloride; acetic acid; dicyclohexyl-carbodiimide;
In
diethyl ether; nitromethane; toluene;
2: |Knoevenagel Condensation;
DOI:10.1002/chem.201303868