9-(2-naphthyl)-10-((2,5-diphenyl)phenyl)anthracene

Base Information

Chemical Name:9-(2-naphthyl)-10-((2,5-diphenyl)phenyl)anthracene
CAS No.:1271733-30-2
Molecular Formula:C₄₂H₂₈
Molecular Weight:532.684
Hs Code.:

Synonyms:

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Chemical Property of 9-(2-naphthyl)-10-((2,5-diphenyl)phenyl)anthracene

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Technology Process of 9-(2-naphthyl)-10-((2,5-diphenyl)phenyl)anthracene

There total 5 articles about 9-(2-naphthyl)-10-((2,5-diphenyl)phenyl)anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 597554-03-5
10-(2-naphthyl)anthracene-9-boronic acid

: 76129-22-1
2,5-diphenyliodobenzene

: 1271733-30-2
9-(2-naphthyl)-10-((2,5-diphenyl)phenyl)anthracene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; for 12h; Inert atmosphere; Reflux;
DOI:10.1039/c0jm02877k

Reference yield:

: 3460-18-2
1,4-dibromo-2-nitrobenzene

: 1271733-30-2
9-(2-naphthyl)-10-((2,5-diphenyl)phenyl)anthracene

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / Inert atmosphere; Reflux

2: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 5 h / 1551.49 Torr / Inert atmosphere

3: toluene-4-sulfonic acid; potassium iodide; sodium nitrite / water; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; toluene / 12 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; potassium carbonate; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In 1,2-dimethoxyethane; ethanol; water; ethyl acetate; toluene; acetonitrile; 1: Suzuki coupling / 3: Sandmeyer reaction / 4: Suzuki coupling;
DOI:10.1039/c0jm02877k

Reference yield:

: 25176-17-4
2'-amino-p-terphenyl

: 1271733-30-2
9-(2-naphthyl)-10-((2,5-diphenyl)phenyl)anthracene

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid; potassium iodide; sodium nitrite / water; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; toluene / 12 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In water; toluene; acetonitrile; 1: Sandmeyer reaction / 2: Suzuki coupling;
DOI:10.1039/c0jm02877k