Technology Process of C17H23NO3
There total 8 articles about C17H23NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / 7 h / 0 - 20 °C / Inert atmosphere
2: pyridine; methanesulfonyl chloride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
3: alpha AD-mix / Inert atmosphere
4: sodium periodate / Inert atmosphere
With
pyridine; sodium periodate; alpha AD-mix; methanesulfonyl chloride;
In
tetrahydrofuran;
DOI:10.1039/c2ob25727k
- Guidance literature:
-
With
silica-supported sodium periodate;
In
dichloromethane;
Inert atmosphere;
DOI:10.1039/c2ob25727k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; methanesulfonyl chloride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
2: alpha AD-mix / water; acetone / 35 h / 0 - 4 °C / Inert atmosphere
3: silica-supported sodium periodate / dichloromethane / Inert atmosphere
With
pyridine; alpha AD-mix; methanesulfonyl chloride;
In
tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1039/c2ob25727k