Technology Process of C27H39N7O10
There total 5 articles about C27H39N7O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; sodium methylate;
In
methanol;
at 20 ℃;
for 1.5h;
DOI:10.1021/bc100394k
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 1.5 h / 0 °C / Inert atmosphere
2.1: sodium azide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
3.1: copper diacetate; sodium L-ascorbate / N,N-dimethyl-formamide / 1.5 h / 90 °C / Inert atmosphere; Microwave irradiation; solid phase reaction
3.2: solid phase reaction
4.1: water; sodium methylate / methanol / 1.5 h / 20 °C
With
pyridine; sodium azide; water; sodium methylate; copper diacetate; sodium L-ascorbate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/bc100394k
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: copper diacetate; sodium L-ascorbate / N,N-dimethyl-formamide / 1.5 h / 90 °C / Inert atmosphere; Microwave irradiation; solid phase reaction
1.2: solid phase reaction
2.1: water; sodium methylate / methanol / 1.5 h / 20 °C
With
water; sodium methylate; copper diacetate; sodium L-ascorbate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/bc100394k