C₂₅H₄₀O₂

Base Information

Chemical Name:C₂₅H₄₀O₂
CAS No.:1374219-28-9
Molecular Formula:C₂₅H₄₀O₂
Molecular Weight:372.591
Hs Code.:

C<sub>25</sub>H<sub>40</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₄₀O₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₂₅H₄₀O₂

There total 15 articles about C₂₅H₄₀O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374219-27-8
O-(1S,2S,4R)-4-hydroxy-2-[2-methoxy-4-(2-methyloctan-2-yl)phenyl]cyclohexyl S-methyl carbonodithioate

: 24850-33-7
allyltributylstanane

: 1374219-29-0
C₂₂H₃₆O₂

: 1374219-28-9
C₂₅H₄₀O₂

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In benzene; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1002/adsc.201100898

Reference yield:

: 4683-24-3
1,4-dioxa-spiro[4.5]dec-6-en-8-one

: 1374219-29-0
C₂₂H₃₆O₂

: 1374219-28-9
C₂₅H₄₀O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap; iodine; potassium carbonate / tetrahydrofuran; water / 2 h / 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride / 1,2-dimethoxyethane; water / 12 h / 80 °C / Inert atmosphere

3.1: 5%-palladium/activated carbon; hydrogen / ethanol / 3 h / 30 °C / 760.05 Torr

4.1: C₅₅H₅₀Cl₂N₂P₂Ru; potassium tert-butylate; hydrogen / isopropyl alcohol / 12 h / 20 °C / 38002.6 Torr / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

5.2: 0.75 h / 20 °C

5.3: 0.75 h / 20 °C

6.1: hydrogenchloride / tetrahydrofuran; water / 36 h / 20 °C

7.1: sodium tetrahydroborate / methanol / 0.5 h / -78 - 20 °C

8.1: 2,2'-azobis(isobutyronitrile) / benzene / 12 h / 80 °C / Inert atmosphere

With hydrogenchloride; dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); 5%-palladium/activated carbon; C₅₅H₅₀Cl₂N₂P₂Ru; potassium tert-butylate; hydrogen; iodine; sodium hydride; sodium carbonate; potassium carbonate; lithium chloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; water; isopropyl alcohol; benzene; 2.1: Suzuki coupling;
DOI:10.1002/adsc.201100898

Reference yield:

: 1374219-15-4
2-methoxy-4-(2-methyloctan-2-yl)phenylboronic acid

: 1374219-29-0
C₂₂H₃₆O₂

: 1374219-28-9
C₂₅H₄₀O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride / 1,2-dimethoxyethane; water / 12 h / 80 °C / Inert atmosphere

2.1: 5%-palladium/activated carbon; hydrogen / ethanol / 3 h / 30 °C / 760.05 Torr

3.1: C₅₅H₅₀Cl₂N₂P₂Ru; potassium tert-butylate; hydrogen / isopropyl alcohol / 12 h / 20 °C / 38002.6 Torr / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

4.2: 0.75 h / 20 °C

4.3: 0.75 h / 20 °C

5.1: hydrogenchloride / tetrahydrofuran; water / 36 h / 20 °C

6.1: sodium tetrahydroborate / methanol / 0.5 h / -78 - 20 °C

7.1: 2,2'-azobis(isobutyronitrile) / benzene / 12 h / 80 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); 5%-palladium/activated carbon; C₅₅H₅₀Cl₂N₂P₂Ru; potassium tert-butylate; hydrogen; sodium hydride; sodium carbonate; lithium chloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; water; isopropyl alcohol; benzene; 1.1: Suzuki coupling;
DOI:10.1002/adsc.201100898