[Cr(N,N'-dibenzyl-2-amino-4-iminopent-2-ene(-1H))2]

Base Information

Chemical Name:[Cr(N,N'-dibenzyl-2-amino-4-iminopent-2-ene(-1H))2]
CAS No.:1224198-11-1
Molecular Formula:C₃₈H₄₂CrN₄
Molecular Weight:606.774
Hs Code.:

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Chemical Property of [Cr(N,N'-dibenzyl-2-amino-4-iminopent-2-ene(-1H))2]

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Technology Process of [Cr(N,N'-dibenzyl-2-amino-4-iminopent-2-ene(-1H))2]

There total 2 articles about [Cr(N,N'-dibenzyl-2-amino-4-iminopent-2-ene(-1H))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: CrCl₂(THF)(x)

: 1219501-76-4
[Li(tetrahydrofuran)(N,N'-dibenzyl-2-amino-4-iminopent-2-ene(-1H))]

: 1224198-11-1
[Cr(N,N'-dibenzyl-2-amino-4-iminopent-2-ene(-1H))2]

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; (N2); using Schlenk techniques; dissolving of CrCl2(THF)(x) in THF, addn. of soln. of ((PhCH2NCMe)2CH)Li(THF) in THF, stirring overnight at roomtemp.; evapn. of solvent, extn. with Et2O, filtration, concn., cooling to -30°C, crystn., elem. anal.;
DOI:10.1021/om100144y

Reference yield: 26.0%

: 6099-39-4,21932-10-5
N,N'-di(benzyl)-2-amino-4-iminopent-2-ene

: 10025-73-7,16284-59-6
chromium(III) chloride

: 1224198-11-1
[Cr(N,N'-dibenzyl-2-amino-4-iminopent-2-ene(-1H))2]

Guidance literature:: With C₆H₅Li; In tetrahydrofuran; dibutyl ether; byproducts: LiCl; (N2); using Schlenk techniques; suspending of CrCl3 in THF, cooling to -78°C, addn. dropwise of soln. of PhLi in dibutyl ether, stirring for 5 h at -78°C, addn. of soln. of ((PhCH2NCMe)2CH)H in THF;, warming to room temp. overnight; removal of solvent in vac., extn. with Et2O, filtration, concn., coolingat -30°C, crystn.;
DOI:10.1021/om100144y