C₁₄H₁₄FNO₄S

Base Information

Chemical Name:C₁₄H₁₄FNO₄S
CAS No.:1403681-75-3
Molecular Formula:C₁₄H₁₄FNO₄S
Molecular Weight:311.334
Hs Code.:

C<sub>14</sub>H<sub>14</sub>FNO<sub>4</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₄FNO₄S

Chemical Property:

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Technology Process of C₁₄H₁₄FNO₄S

There total 5 articles about C₁₄H₁₄FNO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1403681-49-1
4-(4-ethyl-2-methoxyphenoxy)-3-fluorobenzenesulfonamide

: 1403681-75-3
C₁₄H₁₄FNO₄S

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - -20 ℃; Inert atmosphere;
DOI:10.1021/jm301113w

Reference yield:

: 369-34-6
3,4-difluoronitrobenzene

: 1403681-75-3
C₁₄H₁₄FNO₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / acetonitrile / 2 h / 80 °C

2.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C / Inert atmosphere

3.1: sodium nitrite; acetic acid; hydrogenchloride / acetonitrile / 0.5 h / 0 °C / Inert atmosphere; Darkness

3.2: 3.5 h / 0 - 50 °C / Inert atmosphere

4.1: ammonia / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: boron tribromide / dichloromethane / -78 - -20 °C / Inert atmosphere

With hydrogenchloride; palladium on activated charcoal; ammonia; hydrogen; boron tribromide; acetic acid; potassium hydroxide; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jm301113w

Reference yield:

: 4-ethyl-2-methoxy-1-(2-nitrophenoxy)benzene

: 1403681-75-3
C₁₄H₁₄FNO₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C / Inert atmosphere

2.1: sodium nitrite; acetic acid; hydrogenchloride / acetonitrile / 0.5 h / 0 °C / Inert atmosphere; Darkness

2.2: 3.5 h / 0 - 50 °C / Inert atmosphere

3.1: ammonia / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / -78 - -20 °C / Inert atmosphere

With hydrogenchloride; palladium on activated charcoal; ammonia; hydrogen; boron tribromide; acetic acid; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jm301113w