C₂₀H₁₆O₂

Base Information

Chemical Name:C₂₀H₁₆O₂
CAS No.:1411841-00-3
Molecular Formula:C₂₀H₁₆O₂
Molecular Weight:288.346
Hs Code.:

C<sub>20</sub>H<sub>16</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₀H₁₆O₂

Chemical Property:

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Technology Process of C₂₀H₁₆O₂

There total 4 articles about C₂₀H₁₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(2-methylphenyl)-3-(trimethylsilyl)prop-2-yn-1-ol

: 1411841-00-3
C₂₀H₁₆O₂

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / methanol / 2 h / 20 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

3: 4-methoxybenzoic acid; trans-di(1-acetato)bis[5-(diphenyl-phosphino)naphth-1-yl]dipalladium(II) / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

4: 1,2-dichloro-ethane / 20 °C / Inert atmosphere

With trans-di(1-acetato)bis[5-(diphenyl-phosphino)naphth-1-yl]dipalladium(II); potassium carbonate; Dess-Martin periodane; 4-methoxybenzoic acid; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol302586m

Reference yield:

: 139416-71-0
1-(o-tolyl)prop-2-yn-1-ol

: 1411841-00-3
C₂₀H₁₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

2: 4-methoxybenzoic acid; trans-di(1-acetato)bis[5-(diphenyl-phosphino)naphth-1-yl]dipalladium(II) / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

3: 1,2-dichloro-ethane / 20 °C / Inert atmosphere

With trans-di(1-acetato)bis[5-(diphenyl-phosphino)naphth-1-yl]dipalladium(II); Dess-Martin periodane; 4-methoxybenzoic acid; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol302586m

Reference yield:

: 529-20-4
2-methylphenyl aldehyde

: 1411841-00-3
C₂₀H₁₆O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 20 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 2 h / 20 °C / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: 4-methoxybenzoic acid; trans-di(1-acetato)bis[5-(diphenyl-phosphino)naphth-1-yl]dipalladium(II) / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

5.1: 1,2-dichloro-ethane / 20 °C / Inert atmosphere

With n-butyllithium; trans-di(1-acetato)bis[5-(diphenyl-phosphino)naphth-1-yl]dipalladium(II); potassium carbonate; Dess-Martin periodane; 4-methoxybenzoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol302586m