C₁₈H₁₂N₂O₇

Base Information

Chemical Name:C₁₈H₁₂N₂O₇
CAS No.:1450663-80-5
Molecular Formula:C₁₈H₁₂N₂O₇
Molecular Weight:368.302
Hs Code.:

C<sub>18</sub>H<sub>12</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₂N₂O₇

Chemical Property:

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Technology Process of C₁₈H₁₂N₂O₇

There total 6 articles about C₁₈H₁₂N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3162-29-6
1-(benzo[d][1,3]dioxol-6-yl)ethanone

: 1450663-80-5
C₁₈H₁₂N₂O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: nitric acid; acetic acid / 2.5 h / 0 - 20 °C

2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / -5 °C

2.2: 24 h / 20 °C

3.1: potassium carbonate / acetonitrile / 3 h / 0 - 20 °C

4.1: sodium tetrahydroborate / methanol / 3.5 h / 0 - 20 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

6.1: trifluoroacetic acid; water

With aluminum (III) chloride; sodium tetrahydroborate; di-isopropyl azodicarboxylate; water; nitric acid; potassium carbonate; acetic acid; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; acetonitrile; 5.1: |Mitsunobu Displacement;
DOI:10.1002/cplu.201200251

Reference yield:

: 1450663-81-6
1-(4,5-dihydroxy-2-nitrophenyl)ethanone

: 1450663-80-5
C₁₈H₁₂N₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 3 h / 0 - 20 °C

2: sodium tetrahydroborate / methanol / 3.5 h / 0 - 20 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

4: trifluoroacetic acid; water

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; water; potassium carbonate; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; acetonitrile; 3: |Mitsunobu Displacement;
DOI:10.1002/cplu.201200251

Reference yield:

: C₁₂H₁₅NO₇

: 1450663-80-5
C₁₈H₁₂N₂O₇

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 3.5 h / 0 - 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

3: trifluoroacetic acid; water

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; water; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; 2: |Mitsunobu Displacement;
DOI:10.1002/cplu.201200251