6-(2-acetoxy-4-methylphenyl)-2-heptanone

Base Information

Chemical Name:6-(2-acetoxy-4-methylphenyl)-2-heptanone
CAS No.:162708-32-9
Molecular Formula:C₁₆H₂₂O₃
Molecular Weight:262.349
Hs Code.:

Synonyms:

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Chemical Property of 6-(2-acetoxy-4-methylphenyl)-2-heptanone

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Technology Process of 6-(2-acetoxy-4-methylphenyl)-2-heptanone

There total 7 articles about 6-(2-acetoxy-4-methylphenyl)-2-heptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 833-85-2
5-(4-methylphenyl)-5-oxopentanoic acid

: 162708-32-9
6-(2-acetoxy-4-methylphenyl)-2-heptanone

Guidance literature:: Multi-step reaction with 7 steps

1: Mg / tetrahydrofuran; diethyl ether / 24 h rt, 2 h reflux

2: p-TsOH / benzene / 6 h / Heating

3: 97 percent / H₂ / 10percent Pd-C / ethyl acetate

4: 66 percent / P₂O₅, MeSO₂OH / 24 h / Ambient temperature

5: 83 percent / diethyl ether / 24 h / Ambient temperature

6: 35percent H₂O₂, concd. H₂SO₄ / tetrahydrofuran / 12 h / Ambient temperature

7: pyridine / 6 h

With methanesulfonic acid; sulfuric acid; hydrogen; dihydrogen peroxide; phosphorus pentoxide; toluene-4-sulfonic acid; magnesium; palladium on activated charcoal; In tetrahydrofuran; pyridine; diethyl ether; ethyl acetate; benzene;
DOI:10.1016/0040-4020(94)00942-N

Reference yield:

: 162708-27-2
(E)-5-(4-methylphenyl)-4-hexenoic acid

: 162708-32-9
6-(2-acetoxy-4-methylphenyl)-2-heptanone

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / H₂ / 10percent Pd-C / ethyl acetate

2: 66 percent / P₂O₅, MeSO₂OH / 24 h / Ambient temperature

3: 83 percent / diethyl ether / 24 h / Ambient temperature

4: 35percent H₂O₂, concd. H₂SO₄ / tetrahydrofuran / 12 h / Ambient temperature

5: pyridine / 6 h

With methanesulfonic acid; sulfuric acid; hydrogen; dihydrogen peroxide; phosphorus pentoxide; palladium on activated charcoal; In tetrahydrofuran; pyridine; diethyl ether; ethyl acetate;
DOI:10.1016/0040-4020(94)00942-N

Reference yield:

: 5-Hydroxy-5-p-tolyl-hexanoic acid

: 162708-32-9
6-(2-acetoxy-4-methylphenyl)-2-heptanone

Guidance literature:: Multi-step reaction with 6 steps

1: p-TsOH / benzene / 6 h / Heating

2: 97 percent / H₂ / 10percent Pd-C / ethyl acetate

3: 66 percent / P₂O₅, MeSO₂OH / 24 h / Ambient temperature

4: 83 percent / diethyl ether / 24 h / Ambient temperature

5: 35percent H₂O₂, concd. H₂SO₄ / tetrahydrofuran / 12 h / Ambient temperature

6: pyridine / 6 h

With methanesulfonic acid; sulfuric acid; hydrogen; dihydrogen peroxide; phosphorus pentoxide; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; pyridine; diethyl ether; ethyl acetate; benzene;
DOI:10.1016/0040-4020(94)00942-N