chloro(η4-1,5-cyclooctadiene)[methyl 2-R(S)-2'-S(R)-benzyloxycarbonylaminopropionylamino-3-(diphenylphosphanyl)methylpropionate]rhodium(I)

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Chemical Name:chloro(η4-1,5-cyclooctadiene)[methyl 2-R(S)-2'-S(R)-benzyloxycarbonylaminopropionylamino-3-(diphenylphosphanyl)methylpropionate]rhodium(I)
CAS No.:875556-89-1
Molecular Formula:C₃₅H₄₁ClN₂O₅PRh
Molecular Weight:739.053
Hs Code.:

chloro(η4-1,5-cyclooctadiene)[methyl 2-R(S)-2'-S(R)-benzyloxycarbonylaminopropionylamino-3-(diphenylphosphanyl)methylpropionate]rhodium(I)

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Chemical Property of chloro(η4-1,5-cyclooctadiene)[methyl 2-R(S)-2'-S(R)-benzyloxycarbonylaminopropionylamino-3-(diphenylphosphanyl)methylpropionate]rhodium(I)

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Technology Process of chloro(η4-1,5-cyclooctadiene)[methyl 2-R(S)-2'-S(R)-benzyloxycarbonylaminopropionylamino-3-(diphenylphosphanyl)methylpropionate]rhodium(I)

There total 2 articles about chloro(η4-1,5-cyclooctadiene)[methyl 2-R(S)-2'-S(R)-benzyloxycarbonylaminopropionylamino-3-(diphenylphosphanyl)methylpropionate]rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 875557-05-4
2-(2-benzyloxycarbonylamino-propionylamino)-3-diphenylphosphanyl-propionic acid methyl ester

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 875556-89-1
chloro(η4-1,5-cyclooctadiene)[methyl 2-R(S)-2'-S(R)-benzyloxycarbonylaminopropionylamino-3-(diphenylphosphanyl)methylpropionate]rhodium(I)

Guidance literature:: In benzene; (Ar); dropwise addn. of a soln. of ligand in benzene to a soln. of rhodium complex in benzene, stirring at room temp. for 1 h; evapn., recrystn. (ethanol); elem. anal.;
DOI:10.1039/b512653c