(1N-(2-pyridyl-2-methyl)-2-phenylazo anilinate) palladium(II) chloride]

Base Information

• Chemical Name: (1N-(2-pyridyl-2-methyl)-2-phenylazo anilinate) palladium(II) chloride]
• CAS No.: 913059-40-2
• Molecular Formula: C₁₈H₁₅ClN₄Pd
• Molecular Weight: 429.217
• Mol file: 913059-40-2.mol

Synonyms:

Chemical Property of (1N-(2-pyridyl-2-methyl)-2-phenylazo anilinate) palladium(II) chloride]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (1N-(2-pyridyl-2-methyl)-2-phenylazo anilinate) palladium(II) chloride]

There total 1 articles about (1N-(2-pyridyl-2-methyl)-2-phenylazo anilinate) palladium(II) chloride] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

sodium tetrachloropalladate(II) + 1N-(2-pyridyl-2-methyl)-2-phenylazo aniline (913059-36-6) → (1N-(2-pyridyl-2-methyl)-2-phenylazo anilinate) palladium(II) chloride] (913059-40-2)

Guidance literature:

In methanol; methanolic soln. of organic ligand added to methanolic soln. of NaPdCl4;mixture stirred for 5 h; dark solid precipitate separated by filtration; purified by column chromy. using silica gel; eluent benzene-acetonitrile(19:1 v/v)); solvent vaporated; elem. anal.;

DOI:10.1016/j.poly.2006.03.019

upstream raw materials:

1N-(2-pyridyl-2-methyl)-2-phenylazo aniline