6-chloro-7-(4-tolyl)-5,12-diazabenzanthracene

Base Information

• Chemical Name: 6-chloro-7-(4-tolyl)-5,12-diazabenz
• Molecular Formula: C₂₃H₁₅ClN₂
• Molecular Weight: 354.839

Synonyms:

Chemical Property of 6-chloro-7-(4-tolyl)-5,12-diazabenz

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

There total 3 articles about 6-chloro-7-(4-tolyl)-5,12-diazabenzanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-(4-tolyl)-5,12-diazabenzanthracen-6-ol (107263-30-9) → 6-chloro-7-(4-tolyl)-5,12-diazabenzanthracene (107263-32-1)

Guidance literature:

With thionyl chloride; In N,N-dimethyl-formamide; for 1.16667h; Heating;

Reference yield:

4-anilino-quinolin-2-ol (6628-93-9) → 6-chloro-7-(4-tolyl)-5,12-diazabenzanthracene (107263-32-1)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc chloride / 3 h / 285 °C

2: thionyl chloride / dimethylformamide / 1.17 h / Heating

With thionyl chloride; zinc(II) chloride; In N,N-dimethyl-formamide;

Reference yield:

p-Toluic acid (99-94-5) → 6-chloro-7-(4-tolyl)-5,12-diazabenzanthracene (107263-32-1)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc chloride / 3 h / 285 °C

2: thionyl chloride / dimethylformamide / 1.17 h / Heating

With thionyl chloride; zinc(II) chloride; In N,N-dimethyl-formamide;

upstream raw materials:

7-(4-tolyl)-5,12-diazabenzanthracen-6-ol

4-anilino-quinolin-2-ol

p-Toluic acid

Downstream raw materials:

6-anilino-7-(4-tolyl)-5,12-diazabenzanthracene

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